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Revista de Chimie (Rev. Chim.), Year 2015, Volume 66, Issue 8,





Mircea Niculescu, Angela Magda, Marius Jurca, Liviu Costea, Vasile PodE
Thermal and Kinetic Studies of the Polynuclear Coordination Compound Obtained Through the Reaction of 1,3-propanediol with Ni(NO3)2 . 6 H2O

Abstract:

Our paper presents the experimental results of the thermal analysis of Ni(II)-polynuclear coordination compound having as ligand 3-hydroxypropionate anion (L), which is oxidation product of 1,3-propanediol. The reaction between 1,3-propanediol and Ni(NO3)2×6H2O occurs, under specific working conditions, with the oxidation of 1,3-propanediol to the 3-hydroxypropionate anion (HO-CH2-CH2-COO-). The thermal properties of the synthesized polynuclear coordination compound have been investigated by TG, DTG and DTA. The kinetic analysis of the nonisothermal data has been carried out through the isoconversional method. The simple oxide obtained through thermolysis was characterized by IR, X-ray spectroscopy, scanning electron microscopy (SEM) and elemental analysis. Keywords: 1,3-propanediol; Ni(NO3)2 . 6H2O; polynuclear coordination compound, 3-hydroxypropionate, thermal analysis


Issue: 2015, Volume 66, Issue 8
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