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Revista de Chimie (Rev. Chim.), Year 2009, Volume 60, Issue 9,





Ioana Ramona SALAGEAN, Geza BANDUR, Patrick MARTIN, Vincent LEQUART, Lucian Mircea RUSNAC
Synthesis and Characterization of Some Carbohydrate Based Monomers

Abstract:

Carbohydrate based polymers have emerged as exciting topics of the polymer research, due to a worldwide focus on sustainable materials. The biodegradable polymers are indispensable in the modern society and their importance is continuously growing. We report here the synthesis and characterization of a new class of biodegradable copolymers derived from monosaccharides. The synthesis of glycomonomers 3-O-acryloyl-1,2:5,6-di-O-isopropylidene-a-glucofuranose (ADAG), and 1-O-acryloyl-2,3:5,6-di-O-isopropylidene-a-mannofuranose (ADAM) was accomplished by the reaction of the free OH of 1,2:5,6-di-O-isopropylidene-a-glucofuranose (DAG), and 2,3:5,6-di-O-isopropylidene-a-mannofuranose (DAM) with acryloyl chloride. After purification, the resulting unsaturated derivatives of glucose and mannose were characterized by FT IR and NMR spectroscopy and then were copolymerized with some acrylates and methacrylates. The influences of the nature of initiators were investigated using DSC analysis. Key words: carbohydrate, biomaterials, glycopolymers


Issue: 2009, Volume 60, Issue 9
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